The synthesis of multilayer graphene materials by the fluorination of carbon nanodiscs/nanocones

Yasser Ahmad; Elodie Disa; Marc Dubois; Katia Guérin; Vincent Dubois; Wei Zhang; Pierre Bonnet; Francis Masin; Loïc Vidal; Dimitri A. Ivanov; André Hamwi

doi:10.1016/j.carbon.2012.04.034

The synthesis of multilayer graphene materials by the fluorination of carbon nanodiscs/nanocones

Yasser Ahmad
, Elodie Disa
, Marc Dubois^*
, Katia Guérin
, Vincent Dubois
, Wei Zhang
, Pierre Bonnet
, Francis Masin
, Loïc Vidal
, Dimitri A. Ivanov
, André Hamwi

^*此作品的通讯作者

杭州国际创新研究院

Université Clermont Auvergne
CNRS, UMR 6296, Institut de Chimie de Clermont-Ferrand
Université libre de Bruxelles
Institut de Sciences des Matériaux de Mulhouse

科研成果: 期刊稿件 › 文章 › 同行评审

25 引用（Scopus）

摘要

Multilayer carbonaceous nanomaterial has been synthesized using a two-step process: carbon nanodiscs/nanocones were fluorinated using either the direct reaction with pure F ₂ gas or the thermal decomposition of solid fluorinating agent (TbF ₄). Then the fluorinated parts were removed by treatment at 600 °C in air. When the fluorine atoms are homogenously dispersed, using fluorination by TbF ₄, thinning due to thermal defluorination results in multilayer materials with 7-10 nm of thickness and 400-500 nm of width. Such resulting materials and the fluorinated precursors have been characterized by solid state NMR, TGA, XRD, SEM, TEM, AFM and Raman spectroscopy.

源语言	英语
页（从-至）	3897-3908
页数	12
期刊	Carbon
卷	50
期	10
DOI	https://doi.org/10.1016/j.carbon.2012.04.034
出版状态	已出版 - 8月 2012

访问文件

10.1016/j.carbon.2012.04.034

其它文件与链接

链接到 Scopus 的出版物

引用此

@article{3f69d96cb68a45c887bdb806f487ff81,

title = "The synthesis of multilayer graphene materials by the fluorination of carbon nanodiscs/nanocones",

abstract = "Multilayer carbonaceous nanomaterial has been synthesized using a two-step process: carbon nanodiscs/nanocones were fluorinated using either the direct reaction with pure F 2 gas or the thermal decomposition of solid fluorinating agent (TbF 4). Then the fluorinated parts were removed by treatment at 600 °C in air. When the fluorine atoms are homogenously dispersed, using fluorination by TbF 4, thinning due to thermal defluorination results in multilayer materials with 7-10 nm of thickness and 400-500 nm of width. Such resulting materials and the fluorinated precursors have been characterized by solid state NMR, TGA, XRD, SEM, TEM, AFM and Raman spectroscopy.",

author = "Yasser Ahmad and Elodie Disa and Marc Dubois and Katia Gu{\'e}rin and Vincent Dubois and Wei Zhang and Pierre Bonnet and Francis Masin and Lo{\"i}c Vidal and Ivanov, \{Dimitri A.\} and Andr{\'e} Hamwi",

year = "2012",

month = aug,

doi = "10.1016/j.carbon.2012.04.034",

language = "英语",

volume = "50",

pages = "3897--3908",

journal = "Carbon",

issn = "0008-6223",

publisher = "Elsevier Ltd",

number = "10",

}

TY - JOUR

T1 - The synthesis of multilayer graphene materials by the fluorination of carbon nanodiscs/nanocones

AU - Ahmad, Yasser

AU - Disa, Elodie

AU - Dubois, Marc

AU - Guérin, Katia

AU - Dubois, Vincent

AU - Zhang, Wei

AU - Bonnet, Pierre

AU - Masin, Francis

AU - Vidal, Loïc

AU - Ivanov, Dimitri A.

AU - Hamwi, André

PY - 2012/8

Y1 - 2012/8

N2 - Multilayer carbonaceous nanomaterial has been synthesized using a two-step process: carbon nanodiscs/nanocones were fluorinated using either the direct reaction with pure F 2 gas or the thermal decomposition of solid fluorinating agent (TbF 4). Then the fluorinated parts were removed by treatment at 600 °C in air. When the fluorine atoms are homogenously dispersed, using fluorination by TbF 4, thinning due to thermal defluorination results in multilayer materials with 7-10 nm of thickness and 400-500 nm of width. Such resulting materials and the fluorinated precursors have been characterized by solid state NMR, TGA, XRD, SEM, TEM, AFM and Raman spectroscopy.

AB - Multilayer carbonaceous nanomaterial has been synthesized using a two-step process: carbon nanodiscs/nanocones were fluorinated using either the direct reaction with pure F 2 gas or the thermal decomposition of solid fluorinating agent (TbF 4). Then the fluorinated parts were removed by treatment at 600 °C in air. When the fluorine atoms are homogenously dispersed, using fluorination by TbF 4, thinning due to thermal defluorination results in multilayer materials with 7-10 nm of thickness and 400-500 nm of width. Such resulting materials and the fluorinated precursors have been characterized by solid state NMR, TGA, XRD, SEM, TEM, AFM and Raman spectroscopy.

UR - https://www.scopus.com/pages/publications/84861586792

U2 - 10.1016/j.carbon.2012.04.034

DO - 10.1016/j.carbon.2012.04.034

M3 - 文章

AN - SCOPUS:84861586792

SN - 0008-6223

VL - 50

SP - 3897

EP - 3908

JO - Carbon

JF - Carbon

IS - 10

ER -

The synthesis of multilayer graphene materials by the fluorination of carbon nanodiscs/nanocones

摘要

访问文件

其它文件与链接

指纹

引用此