Synthesis and the thermal stability of NdOOH nanotubes

Jiaxin He; Fang Liang; Lin Guo

Synthesis and the thermal stability of NdOOH nanotubes

Jiaxin He^*
, Fang Liang
, Lin Guo

^*Corresponding author for this work

School of Chemistry

Beihang University

Research output: Contribution to journal › Article › peer-review

Abstract

The uniform, large-scale, bundles of unbodied NdOOH nanotubes have been synthesized by the improved microemulsion method in the presence of an anionic surfactant, sodium bis (2-ethylhexyl) sulfosuccinate (AOT) in toluene with nitrate neodymium and hydrogen peroxide at a low temperature. The structural and chemical information of the nanotubes was studied using X-ray diffraction (XRD), transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM). The NdOOH nanotubes have diameters about 100 nm and lengths up to 0.5um. The thermal behaviour of the present compounds has been determined by means of thermogravimetry (TG) and differential scanning calorimetry (DSC) techniques. It has demonstrated that the stable Nd₂O₃ would be formed by heating.

Original language	English
Pages (from-to)	272-274
Number of pages	3
Journal	Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering
Volume	36
Issue number	SUPPL. 2
State	Published - Aug 2007

Keywords

AOT
Lanthanon
Microemulsion
NdOOH

Cite this

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title = "Synthesis and the thermal stability of NdOOH nanotubes",

abstract = "The uniform, large-scale, bundles of unbodied NdOOH nanotubes have been synthesized by the improved microemulsion method in the presence of an anionic surfactant, sodium bis (2-ethylhexyl) sulfosuccinate (AOT) in toluene with nitrate neodymium and hydrogen peroxide at a low temperature. The structural and chemical information of the nanotubes was studied using X-ray diffraction (XRD), transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM). The NdOOH nanotubes have diameters about 100 nm and lengths up to 0.5um. The thermal behaviour of the present compounds has been determined by means of thermogravimetry (TG) and differential scanning calorimetry (DSC) techniques. It has demonstrated that the stable Nd2O3 would be formed by heating.",

keywords = "AOT, Lanthanon, Microemulsion, NdOOH",

author = "Jiaxin He and Fang Liang and Lin Guo",

year = "2007",

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language = "英语",

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journal = "Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering",

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TY - JOUR

T1 - Synthesis and the thermal stability of NdOOH nanotubes

AU - He, Jiaxin

AU - Liang, Fang

AU - Guo, Lin

PY - 2007/8

Y1 - 2007/8

N2 - The uniform, large-scale, bundles of unbodied NdOOH nanotubes have been synthesized by the improved microemulsion method in the presence of an anionic surfactant, sodium bis (2-ethylhexyl) sulfosuccinate (AOT) in toluene with nitrate neodymium and hydrogen peroxide at a low temperature. The structural and chemical information of the nanotubes was studied using X-ray diffraction (XRD), transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM). The NdOOH nanotubes have diameters about 100 nm and lengths up to 0.5um. The thermal behaviour of the present compounds has been determined by means of thermogravimetry (TG) and differential scanning calorimetry (DSC) techniques. It has demonstrated that the stable Nd2O3 would be formed by heating.

AB - The uniform, large-scale, bundles of unbodied NdOOH nanotubes have been synthesized by the improved microemulsion method in the presence of an anionic surfactant, sodium bis (2-ethylhexyl) sulfosuccinate (AOT) in toluene with nitrate neodymium and hydrogen peroxide at a low temperature. The structural and chemical information of the nanotubes was studied using X-ray diffraction (XRD), transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HRTEM). The NdOOH nanotubes have diameters about 100 nm and lengths up to 0.5um. The thermal behaviour of the present compounds has been determined by means of thermogravimetry (TG) and differential scanning calorimetry (DSC) techniques. It has demonstrated that the stable Nd2O3 would be formed by heating.

KW - AOT

KW - Lanthanon

KW - Microemulsion

KW - NdOOH

UR - https://www.scopus.com/pages/publications/36248990281

M3 - 文章

AN - SCOPUS:36248990281

SN - 1002-185X

VL - 36

SP - 272

EP - 274

JO - Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering

JF - Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering

IS - SUPPL. 2

ER -

Synthesis and the thermal stability of NdOOH nanotubes

Abstract

Keywords

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