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Synthesis and characterization of a novel microporous aluminophosphate A1PO4- JDF (2A1PO4HOCH2CH2NH2) from alcohol systems

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Abstract

The synthesis of a novel aluminophosphate microporous compound A1PO4-JDF (where J means Jilin University and DF is Davy Faraday Laboratory) containing organic amine in the presence of the template HOCH2CH2NH2 from predominantly nonaqueous media is described. Chemical and elemental analyses disclosed its idealized formula as 2A1PO4 -HOCH2CH2NH2. A1PO4-JDF has been characterized by X-ray powder diffraction (XRD), IR spectroscopy, scanning electron microscopy (SEM), differential thermal analysis (DTA) and thermogravimetry (TG), and magic angle spinning nuclear magnetic resonance (MAS NMR) spectroscopy.

Original languageEnglish
Pages (from-to)1207-1210
Number of pages4
JournalJournal of Materials Chemistry
Volume6
Issue number7
DOIs
StatePublished - 1996
Externally publishedYes

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