Surface microstructure and phase structure of zirconia ceramics under intense pulsed ion beam irradiation

Shijian Zhang; Xiao Yu; Jie Zhang; Vladimir Vasilevich Uglov; Andrey Vladimirovich Stepanov; Xiang Yu; Mofei Xu; Chang Xiong; Yanmei Sun; Gennady Efimovich Remnev; Sha Yan; Xiaoyun Le

doi:10.1016/j.nimb.2023.06.006

Surface microstructure and phase structure of zirconia ceramics under intense pulsed ion beam irradiation

Shijian Zhang
, Xiao Yu
, Jie Zhang
, Vladimir Vasilevich Uglov
, Andrey Vladimirovich Stepanov
, Xiang Yu
, Mofei Xu
, Chang Xiong
, Yanmei Sun
, Gennady Efimovich Remnev
, Sha Yan
, Xiaoyun Le^*

^*Corresponding author for this work

School of Physics

Research output: Contribution to journal › Article › peer-review

3 Scopus citations

Abstract

The surface microstructure and phase structure of zirconia (ZrO₂) ceramics under intense pulsed ion beam (IPIB) irradiation were investigated in this work. Experiments were carried out on TEMP-4M accelerator with peak accelerating voltage, current density, and pulse duration of 220 kV, 150 A/cm², and 80 ns. Micro-cracks with a height of up to 150 nm above the surface were observed and were deduced to be formed by the tensile stress during the shrinking process. The cross-sectional observation indicates that columnar structure thin layer with thickness about 1.23 μm was produced after IPIB irradiation. The GIXRD pattern indicates that obvious preferred orientation in (1 1 0) and (2 0 0) of t-ZrO₂ was occurred in near-surface region after IPIB irradiation. Opposite micro-stress in bulk and near-surface region was revealed by W-H plot after Rietveld refinement. The evolution of mass loss and surface roughness of samples with pulse number was also investigated.

Original language	English
Pages (from-to)	110-128
Number of pages	19
Journal	Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms
Volume	542
DOIs	https://doi.org/10.1016/j.nimb.2023.06.006
State	Published - Sep 2023

Keywords

Intense pulsed ion beam
Phase structure
Rietveld refinement
Surface microstructure

Access to Document

10.1016/j.nimb.2023.06.006

Cite this

Zhang, S., Yu, X., Zhang, J., Uglov, V. V., Stepanov, A. V., Yu, X., Xu, M., Xiong, C., Sun, Y., Remnev, G. E., Yan, S., & Le, X. (2023). Surface microstructure and phase structure of zirconia ceramics under intense pulsed ion beam irradiation. Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, 542, 110-128. https://doi.org/10.1016/j.nimb.2023.06.006

@article{50ca92f3c5054793940df28b0889e5e8,

title = "Surface microstructure and phase structure of zirconia ceramics under intense pulsed ion beam irradiation",

abstract = "The surface microstructure and phase structure of zirconia (ZrO2) ceramics under intense pulsed ion beam (IPIB) irradiation were investigated in this work. Experiments were carried out on TEMP-4M accelerator with peak accelerating voltage, current density, and pulse duration of 220 kV, 150 A/cm2, and 80 ns. Micro-cracks with a height of up to 150 nm above the surface were observed and were deduced to be formed by the tensile stress during the shrinking process. The cross-sectional observation indicates that columnar structure thin layer with thickness about 1.23 μm was produced after IPIB irradiation. The GIXRD pattern indicates that obvious preferred orientation in (1 1 0) and (2 0 0) of t-ZrO2 was occurred in near-surface region after IPIB irradiation. Opposite micro-stress in bulk and near-surface region was revealed by W-H plot after Rietveld refinement. The evolution of mass loss and surface roughness of samples with pulse number was also investigated.",

keywords = "Intense pulsed ion beam, Phase structure, Rietveld refinement, Surface microstructure",

author = "Shijian Zhang and Xiao Yu and Jie Zhang and Uglov, \{Vladimir Vasilevich\} and Stepanov, \{Andrey Vladimirovich\} and Xiang Yu and Mofei Xu and Chang Xiong and Yanmei Sun and Remnev, \{Gennady Efimovich\} and Sha Yan and Xiaoyun Le",

note = "Publisher Copyright: {\textcopyright} 2023 Elsevier B.V.",

year = "2023",

month = sep,

doi = "10.1016/j.nimb.2023.06.006",

language = "英语",

volume = "542",

pages = "110--128",

journal = "Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms",

issn = "0168-583X",

publisher = "Elsevier B.V.",

}

Zhang, S, Yu, X, Zhang, J, Uglov, VV, Stepanov, AV, Yu, X, Xu, M, Xiong, C , Sun, Y, Remnev, GE, Yan, S & Le, X 2023, 'Surface microstructure and phase structure of zirconia ceramics under intense pulsed ion beam irradiation', Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms, vol. 542, pp. 110-128. https://doi.org/10.1016/j.nimb.2023.06.006

TY - JOUR

T1 - Surface microstructure and phase structure of zirconia ceramics under intense pulsed ion beam irradiation

AU - Zhang, Shijian

AU - Yu, Xiao

AU - Zhang, Jie

AU - Uglov, Vladimir Vasilevich

AU - Stepanov, Andrey Vladimirovich

AU - Yu, Xiang

AU - Xu, Mofei

AU - Xiong, Chang

AU - Sun, Yanmei

AU - Remnev, Gennady Efimovich

AU - Yan, Sha

AU - Le, Xiaoyun

PY - 2023/9

Y1 - 2023/9

N2 - The surface microstructure and phase structure of zirconia (ZrO2) ceramics under intense pulsed ion beam (IPIB) irradiation were investigated in this work. Experiments were carried out on TEMP-4M accelerator with peak accelerating voltage, current density, and pulse duration of 220 kV, 150 A/cm2, and 80 ns. Micro-cracks with a height of up to 150 nm above the surface were observed and were deduced to be formed by the tensile stress during the shrinking process. The cross-sectional observation indicates that columnar structure thin layer with thickness about 1.23 μm was produced after IPIB irradiation. The GIXRD pattern indicates that obvious preferred orientation in (1 1 0) and (2 0 0) of t-ZrO2 was occurred in near-surface region after IPIB irradiation. Opposite micro-stress in bulk and near-surface region was revealed by W-H plot after Rietveld refinement. The evolution of mass loss and surface roughness of samples with pulse number was also investigated.

AB - The surface microstructure and phase structure of zirconia (ZrO2) ceramics under intense pulsed ion beam (IPIB) irradiation were investigated in this work. Experiments were carried out on TEMP-4M accelerator with peak accelerating voltage, current density, and pulse duration of 220 kV, 150 A/cm2, and 80 ns. Micro-cracks with a height of up to 150 nm above the surface were observed and were deduced to be formed by the tensile stress during the shrinking process. The cross-sectional observation indicates that columnar structure thin layer with thickness about 1.23 μm was produced after IPIB irradiation. The GIXRD pattern indicates that obvious preferred orientation in (1 1 0) and (2 0 0) of t-ZrO2 was occurred in near-surface region after IPIB irradiation. Opposite micro-stress in bulk and near-surface region was revealed by W-H plot after Rietveld refinement. The evolution of mass loss and surface roughness of samples with pulse number was also investigated.

KW - Intense pulsed ion beam

KW - Phase structure

KW - Rietveld refinement

KW - Surface microstructure

UR - https://www.scopus.com/pages/publications/85163001319

U2 - 10.1016/j.nimb.2023.06.006

DO - 10.1016/j.nimb.2023.06.006

M3 - 文章

AN - SCOPUS:85163001319

SN - 0168-583X

VL - 542

SP - 110

EP - 128

JO - Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms

JF - Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms

ER -

Surface microstructure and phase structure of zirconia ceramics under intense pulsed ion beam irradiation

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this