Abstract
Bi2Te3 nanocrystals with various shapes such as sheet, rag, sheet-rod and rod shapes were synthesized via a solvothermal process based on the reaction between BiCl3 and Te in N,N -dimethylformamide at 100-180 °C at the present of organic addition and/or reducing agent. The products were characterized by X-ray diffraction, X-ray fluorescence (XRF) analysis, inductively coupled plasma-atomic emission spectroscopy (ICP-AES) and transmission electron microscopy (TEM). KBH4 was used as a reducing agent. Organic additive plays a key role in the formation of the lamellar structures. A possible formation mechanism is proposed.
| Original language | English |
|---|---|
| Pages (from-to) | 410-415 |
| Number of pages | 6 |
| Journal | Chemical Physics Letters |
| Volume | 374 |
| Issue number | 3-4 |
| DOIs | |
| State | Published - 11 Jun 2003 |
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