Abstract
ZrB2-SiC nanocomposite ceramics toughened by ZrO2 fiber were fabricated by spark plasma sintering (SPS) at 1700°C. The content of ZrO2 fiber incorporated into the ZrB2-SiC nanocomposites ranged from 5mass% to 20mass%. The content, microstructure, and phase transformation of ZrO2 fiber exhibited remarkable effects on the fracture toughness of the ZrO2(f)/ZrB2-SiC composites. Fracture toughness of the composites greatly improved to a maximum value of 6.56MPam1/2±0.3MPam1/2 by the addition of 15mass% of ZrO2 fiber. The microstructure of the ZrO2 fiber exhibited certain alterations after the SPS process, which enhanced crack deflection and crack bridging and affected fracture toughness. Some microcracks were induced by the phase transformation from t-ZrO2 to m-ZrO2, which was also an important reason behind the improvement in toughness.
| Original language | English |
|---|---|
| Pages (from-to) | 808-813 |
| Number of pages | 6 |
| Journal | Materials and Design |
| Volume | 49 |
| DOIs | |
| State | Published - Aug 2013 |
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