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An improved convective self-assembly method for the fabrication of binary colloidal crystals and inverse structures

  • Zhongyu Cai
  • , Jinghua Teng
  • , Yong Wan
  • , X. S. Zhao*
  • *Corresponding author for this work
  • National University of Singapore
  • Agency for Science, Technology and Research, Singapore
  • Qingdao University
  • University of Queensland

Research output: Contribution to journalArticlepeer-review

Abstract

We report an improved convective self-assembly method for the fabrication of highly ordered, crack-free binary colloidal crystals (BCCs) and the associated inverse structures in large domains at length scales of several centimeters. With this method, BCCs can be fabricated in a non-close packed pattern and binary inverse opal films can be obtained over a centimeter scale. The presence of tetraethyl orthosilicate (TEOS) sol in the self-assembly system was found to play a significant role in the resultant structures. The pseudostop band positions are adjustable via varying the number ratio of small to large polystyrene (PS) spheres. At a given TEOS-to-PS ratio, the binary inverse opal film thickness was controllable by varying the colloidal volume fraction with an upper thickness threshold (>16 layers).

Original languageEnglish
Pages (from-to)42-50
Number of pages9
JournalJournal of Colloid and Interface Science
Volume380
Issue number1
DOIs
StatePublished - 15 Aug 2012
Externally publishedYes

Keywords

  • Binary colloidal crystals
  • Binary inverse opals
  • Convective self-assembly
  • Crack-free
  • Macroporous

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